Netzsch sample correction 측정 방법

Standard Test Method for Steady-State Thermal Transmission Properties by Mean of the Heat Flow Meter Apparatus, ASTM C518-02 American Society for Testing and Materials; 2004.

Bomberg, M., Solvason, K.R.. (Comments on Calibration and Design of a Heat Flow Meter, STP 789 American Society for Testing and Materials(ASTM); 1983). 277-292.

Jang, C.W., Shim, C.S., Song, H.C., Song, C.Y.. (Study on Cryogenic Behavior of Reinforced Polyurethane Foam for Membrane Type LNG Carrier, Journal of Ocean Engineering and Technology, 2013). 27(1):74-79 10.5574/KSOE.2013.27.1.074.


Kim, B.S., Kim, J.H., Kim, Y.J., Cho, H.H.. (Fabrication and Calibration of Micro Heat Flux Sensor for Heat Flux Measurement Proceedings of KSME 2005 Autumn Annual Meeting Yongpyeong Korea: 2005). 195-199.

Kim, J.G., Kim, Y.M., Kim, C.S.. (A Study on Unsteady Temperature Distribution Analysis of Moss Type LNG Carrier by Insulation System, Journal of Ocean Engineering and Technology, 1997). 11(4):159-168.

Lee, J.H., Kim, Y.J., Hwang, S.Y.. (Numerical Model of Heat Diffusion and Evaporation by LNG Leakage at Membrane Insulation, Journal of Ocean Engineeing and Technology, 2014). 28(6):517-526 10.5574/KSOE.2014.28.6.517.


Lee, J.S., Kim, K.S., Kim, Y.I., Yoo, C.H., Park, J.I., Kang, B.H.. (Fatigue Strength Assessment of High Manganese Steel for LNG CCS, Journal of the Society of Naval Architects of Korea, 2014). 51(3):246-253 10.3744/SNAK.2014.51.3.246.


Lee, J.S., Kim, K.S., Kim, Y.I., Yoo, C.H., You, W.H.. (An Experimental Study on Fatigue Performance of Cryogenic metallic materials for IMO type B tank, International Journal of Naval Architecture and Ocean Engineering, 2013). 5(4):580-597.


Heat Flow Meter 2014). [Online] (Updated February 2014), Available at: <//www.netzsch.com/> [Accessed October 2014].

Han, K.C., Hwang, S.W., Cho, J.R., Kim, J.S., Yoon, J.W., Lim, O.K., Lee, S.B.. (Astudy on the Boil-Off Rate Prediction of LNG Cargo Containment Filled with Insulation Powders, Journal of the Computational Structural Engineering Institute of Korea, 2011). 24(2):193-200.

Haruyama, T.. (Performance of Peltier Elements as a Cryogenic Heat Flux Sensor at Temperatures down to 60K, Cryogenics, 2001). 41, 335-339 10.1016/S0011-2275(01)00081-9.


Thermal Conductivity and Resistance 2005). [Online] (Updated July 2005) Available at: <//www.usask.ca/> [Accessed October 2014].

Yang, H.C., Song, C.H., Kim, M.H.. (Development of Micro-machined Heat Flux Sensor by Using MEMS Technology Proceedings of KSME 2004 Spring Annual Meeting Pyeong-chang Korea: 2004). 1364-1369.

정보제공 : ZEUS 장비활용종합포털(www.zeus.go.kr)

열중량분석기

Simultaneous Thermal Analyzer

GBTP No.시설장비등록번호보유기관담당자연락처이메일
GBREMS-09-0024
NFEC-2013-08-181692
(재)포항금속소재산업진흥원

장비정보

모델명제작사취득일자취득금액표준분류활용용도장비위치장비설명구성 및 기능사용/활용예이용안내유의사항
STA 449 F3 Netzsch
2013-06-30 140,000,000원
물리적측정장비 > 온도/열/습도/수분측정장비 > 열분석기 시험

F1

- 온도를 증가시켜 일어나는 시료의 무게 변화를 온도 또는 시간의 함수로 기록한다.
- TG 곡선을 통해 정해진 온도범위에서 일어나는 물리적인 변화나 화학적인 반응의 결과에 따른 주어진 화합물이나 물질의 특징을 관찰한다.
설치장소: 포항금속소재산업진흥원 1층 120호
1) Temperature Range : RT(Room Temperature) ~ 1300°C
2) Furnace type : Vertical, top-loading to allow easy handling and to support the natural gas path and avoid condensation problems
3) Furnace hoist : Motorized single and double furnace hoists available
4) Simultaneous installed two different furnaces and easily changed by the operator
5) Vacuum tight : Down to 10-2 mbar
6) Auto-vac : Available
7) Minimum oxygen partial pressure : < 1 ppm (with OTSTM)
8) MFC Gas flow : 3 purges input, 0 … 250 ml/min or more
9) Metal housed internal MFC control system
10) Stainless gas tubing system
11) MFC control accuracy : 0.25 % or better
12) Temperature resolution : 0.001°C or better
13) Temperature accuracy : 0.3°C or better
14) TG measuring range : Max. 35 g (35000 mg)
15) TG sensitivity : 1 μg
16) Balance noise : +/-2 digits
17) Balance drift : < 5 μg/hour
18) Sample volume : 5 cm3
19) Corrosive gas : Available
20) Evolved gas analysis : Tailor made QMS and/or FTIR(Fourier transform infrared spectroscopy) couplings(Available)
21) Temperature modulated software (TM-DSC)
22) Baseline correction software Beflat
23) DSC correction is available
24) User exchangeable furnaces must be available
- 시편의 무게변화가 없는 온도를 측정하여 그 물질의 안정성을 판단할 수 있다.
- 가혹한 부식 환경(수증기 및 부식가스)에 장시간 노출시켜 중량변화를 측정하여 산화속도 및 안정성을 판단한다.

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